In-situ Raman Spectroelectrochemical Cell Model:EC-RM3S
In-situ Raman Spectroelectrochemical Cell Model:EC-RM3S
In-situ Raman Spectroelectrochemical Cell Model:EC-RM3S

CNB-12-EC-RM3S

In-situ Raman Spectroelectrochemical Cell Model:EC-RM3S

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Model

Product Overview

The EC-RM3S is an upgraded version of the EC-RM3 In-situ Raman Spectroelectrochemical Cell. It retains the membrane-separated three-chamber configuration and direct Raman access of the EC-RM3, while incorporating a serpentine flow channel within the gas chamber. The extended gas flow path increases the contact time between the reactant gas and the catalyst layer, allowing the gas to participate more effectively in the electrochemical reaction.

Key Features 

Serpentine Gas Flow Channel
Extends the gas flow path across the working electrode, enabling controlled reactant delivery

Extended Gas–Catalyst Contact
Increases gas residence time to enhance interaction between the reactant gas and catalyst layer

Enhanced Gas-Fed Interface Control
Promotes effective gas participation during operando Raman investigation of the electrochemical interface

Technical Specifications

Working electrode area 1 cm² (customizable)
WE-Optical window distance < 6 mm
Optical window diameter

Ø37 mm
(effective diameter Ø34 mm)

Chamber structure Three-chamber gas-diffusion configuration with a serpentine flow channel
Working electrode Sheet-type gas-diffusion electrode (e.g., Au, Pt, glassy carbon, ITO, and FTO)
Reference electrode Ag/AgCl or Ag/Ag⁺ electrode
Counter electrode Platinum wire or graphite rod electrode
Cell body materials PEEK + Ti
Optical window material Quartz
Cell body dimensions L99 × W70 × H25 mm


Instrument Compatibility

Raman System Compatibility
Compatible with commercial Raman microscope systems, including Renishaw (inVia Qontor), HORIBA (LabRAM HR Evolution and iHR550), and Ocean Optical Instruments (HRS-5A).

Potentiostat Compatibility
Compatible with commercial three-electrode electrochemical workstations, including CH Instruments (CHI660E, CHI760E, and CHI1140C), Bio-Logic (VMP3), and Corrtest Instruments (CS350M).

Published Application Example

In Situ SERS Monitoring of CO₂ Electroreduction
The cell used in this study, supplied by Beyond Battery under product code EC-RM3S, features a gas-fed flow-cell configuration. It was used to investigate copper electrodes with different densities of Cu(100)/(111) grain boundaries during CO₂ electroreduction in a neutral electrolyte.Catalyst-coated gas-diffusion layers served as the working electrodes, while Ag/AgCl and platinum wire were used as the reference and counter electrodes, respectively. In situ SERS monitoring tracked Cu–OH and adsorbed *CO species, linking hydroxyl-rich grain boundaries to enhanced ethylene selectivity.

Demonstrated EC-RM3S Capabilities

  • Operando SERS monitoring in a gas-fed flow-cell configuration
  • Compatibility with catalyst-coated gas-diffusion electrodes
  • Tracking of Cu–OH and adsorbed *CO surface species

Application Studies
Additional application studies are underway.

Product Identification Note: EC-RM3S is the Beyond Battery product code for the same cell reported in the cited publication. The original article uses a different product designation.