{"product_id":"in-situ-xrd-electrochemical-cell-model-ec-xrd1","title":"In-situ XRD Electrochemical Cell (Three-Electrode System), Model: EC-XRD1","description":"\u003ch3 class=\"PDq2pG_selectionAnchorContainer\"\u003eEC-XRD1 \u003cspan class=\"PDq2pG_selectionAnchor\"\u003e\u003c\/span\u003eIn-situ XRD Electrochemical Cell\u003c\/h3\u003e\n\u003cp\u003eA compact three-electrode cell for operando XRD monitoring of electrochemical phase and structural evolution.\u003c\/p\u003e\n\u003ch3\u003eProduct Overview\u003c\/h3\u003e\n\u003cp\u003eThe EC-XRD1 provides direct X-ray access to an interchangeable disk working electrode through an X-ray-transparent beryllium (Be) window while maintaining three-electrode electrochemical control. Its compact flow-compatible design supports both syringe filling and external electrolyte circulation, making it suitable for tracking phase transformations and structural evolution of electrode materials under applied electrochemical conditions.\u003c\/p\u003e\n\u003ch3\u003e\n\u003cspan\u003eTechnical Specifications\u003c\/span\u003e\u003cbr\u003e\n\u003c\/h3\u003e\n\u003ctable style=\"width: 100%;\"\u003e\n\u003ctbody\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eWE-optical window distance\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003e\u0026lt; 3 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eOptical window diameter\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003eØ25 mm (effective diameter Ø20 mm)\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eChamber structure\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003eSingle-chamber\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eElectrode system\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003eThree-electroder\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eWorking electrode\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003eØ5 mm glassy carbon disk electrode (standard); Au, Pt, Ag, graphite, or pyrolytic graphite disk electrodes (optional)\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eReference electrode\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003eAg\/AgCl or Ag\/Ag⁺ electrode\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eCounter electrode\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003eØ1 mm Platinum wire electrode\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eCell body material\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003ePEEK + Ti\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eOptical window material\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003eBeryllium (Be)\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 26.591986%;\"\u003eCell body dimensions\u003c\/td\u003e\n\u003ctd style=\"width: 72.344185%;\"\u003eL65 × W65 × H19 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp class=\"PDq2pG_selectionAnchorContainer\"\u003e\u003cem\u003eNote: Solid beryllium is relatively stable and poses low skin-contact risk; avoid inhaling dust or aerosols and wash hands after handling.\u003c\/em\u003e\u003cspan class=\"PDq2pG_selectionAnchor\"\u003e\u003c\/span\u003e\u003c\/p\u003e\n\u003ch3\u003eKey Features\u003c\/h3\u003e\n\u003cp\u003e\u003cstrong\u003eDirect Structural Observation\u003cbr\u003e\u003c\/strong\u003eBe-window access and a short X-ray path enable direct probing of the working-electrode surface\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eFlexible Disk-Electrode Selection\u003cbr\u003e\u003c\/strong\u003eUses a standard Ø5 mm glassy carbon disk and supports interchangeable Au, Pt, Ag, graphite, and pyrolytic graphite disks\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eOperando Phase-Evolution Analysis\u003cbr\u003e\u003c\/strong\u003eEnables potential- and time-dependent monitoring of crystalline phase transformations and structural evolution of electrode materials\u003cbr\u003e\u003c\/p\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0562\/5705\/2832\/files\/EC-XRD1_dimensions_480x480.png?v=1787550562\" alt=\"\" style=\"float: none;\"\u003e\u003cbr\u003e\u003cmeta charset=\"UTF-8\"\u003e\n\u003ch3 class=\"PDq2pG_selectionAnchorContainer\"\u003eInstrument Compatibility\u003cspan class=\"PDq2pG_selectionAnchor\"\u003e\u003c\/span\u003e\n\u003c\/h3\u003e\n\u003cp\u003e\u003cstrong\u003eXRD System Compatibility\u003cbr\u003e\u003c\/strong\u003eCompatible with laboratory X-ray diffractometers that accommodate external electrochemical cells. Measurement geometry, sample-stage clearance, and mounting should be confirmed before use\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003ePotentiostat Compatibility\u003cbr\u003e\u003c\/strong\u003eCompatible with commercial three-electrode potentiostats for electrochemical control during operando XRD measurements\u003c\/p\u003e\n\u003ch3\u003eRepresentative Application Example\u003c\/h3\u003e\n\u003cp\u003e\u003cstrong\u003eOperando XRD Tracking of LiCoO₂ Structural Evolution during OER\u003cbr\u003e\u003c\/strong\u003eA custom-designed three-electrode operando XRD\/XAFS cell was used to track LiCoO₂ structural evolution during OER in 0.1 M KOH. As the potential increased stepwise from 1.1 to 1.7 V versus RHE, the LiCoO₂ (003) peak gradually weakened. New reflections at 12.87° and 25.88° appeared above 1.50 V, indicating K₀.₃CoO₂(H₂O)₀.₄ formation associated with potential-dependent cation intercalation and structural transformation.\u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eDemonstrated Operando XRD Capabilities\u003c\/strong\u003e\u003c\/p\u003e\n\u003cul\u003e\n\u003cli\u003eSimultaneous XRD acquisition and electrochemical control\u003c\/li\u003e\n\u003cli\u003eDetection of potential-dependent crystalline phase transformations\u003c\/li\u003e\n\u003cli\u003eCorrelation of diffraction evolution with applied electrode potential\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003ch3\u003eApplication Studies\u003c\/h3\u003e\n\u003cp\u003eApplication studies using this model are currently underway.\u003cbr\u003e\u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0562\/5705\/2832\/files\/EC-XRD1_c360b192-b769-496a-b6e5-567025277bbb_480x480.png?v=1787550563\" style=\"float: none;\"\u003e\u003cem\u003e.\u003c\/em\u003e\u003c\/p\u003e\n\u003c\/div\u003e","brand":"Beyond Battery","offers":[{"title":"EC-XRD1","offer_id":52891004797088,"sku":"CNB-12-EC-XRD1","price":2059.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0562\/5705\/2832\/files\/EC-XRD1.png?v=1787550861","url":"https:\/\/beyond-battery.com\/en-us\/products\/in-situ-xrd-electrochemical-cell-model-ec-xrd1","provider":"Beyond Battery","version":"1.0","type":"link"}