{"product_id":"in-in-situ-xrd-battery-test-cell-model-xrd-3e","title":"In-situ XRD Battery Test Cell Model: XRD-3E","description":"\u003cdiv class=\"_tableContainer_16hzy_1\" style=\"text-align: start;\"\u003e\n\u003ch3\u003e\n\u003cspan\u003eXRD-3E \u003c\/span\u003e\u003cspan\u003eIn-Situ XRD Battery Test Cell\u003c\/span\u003e\n\u003c\/h3\u003e\n\u003cp class=\"isSelectedEnd\"\u003e\u003cspan\u003eA three-electrode battery test cell for operando XRD monitoring with independent reference-potential measurement.\u003c\/span\u003e\u003c\/p\u003e\n\u003ch3\u003e\u003cspan\u003eProduct Overview\u003c\/span\u003e\u003c\/h3\u003e\n\u003cp class=\"isSelectedEnd\"\u003e\u003cspan\u003eThe XRD-3E is a three-electrode in-situ XRD battery test cell upgraded from the XRD-2E platform. It enables operando structural analysis during charge\/discharge cycling while an independent lithium reference electrode monitors electrode potential. A low-background beryllium window provides direct X-ray access to the electrode stack, while the high-purity titanium body, PEEK insulation, and gold-plated copper tabs support stable, repeatable electrochemical testing.\u003c\/span\u003e\u003c\/p\u003e\n\u003ch3\u003e\u003cspan\u003eKey Features\u003c\/span\u003e\u003c\/h3\u003e\n\u003cp class=\"isSelectedEnd\"\u003e\u003cspan\u003e• \u003c\/span\u003e\u003cstrong\u003e\u003cspan\u003eIndependent Reference-Electrode Monitoring\u003c\/span\u003e\u003c\/strong\u003e\u003cbr\u003e\u003cspan\u003eUses a lithium reference electrode for independent working-electrode potential monitoring during cycling\u003c\/span\u003e\u003c\/p\u003e\n\u003cp class=\"isSelectedEnd\"\u003e\u003cspan\u003e• \u003c\/span\u003e\u003cstrong\u003e\u003cspan\u003eBruker D8-Compatible XRD Measurement\u003c\/span\u003e\u003c\/strong\u003e\u003cbr\u003e\u003cspan\u003eDesigned for use with Bruker D8 X-ray diffractometer systems for operando XRD monitoring during battery cycling\u003c\/span\u003e\u003c\/p\u003e\n\u003cp\u003e\u003cspan\u003e• \u003c\/span\u003e\u003cstrong\u003e\u003cspan\u003eLow-Angle XRD Accessibility\u003c\/span\u003e\u003c\/strong\u003e\u003cbr\u003e\u003cspan\u003eSupports XRD measurements from a minimum operating angle of 3°, enabling broader low-angle access for operando configurations\u003c\/span\u003e\u003c\/p\u003e\n\u003ch3\u003eTechnical Specifications\u003c\/h3\u003e\n\u003ctable\u003e\n\u003cthead\u003e\n\u003ctr\u003e\n\u003cth\u003e\u003cstrong\u003eParameter\u003c\/strong\u003e\u003c\/th\u003e\n\u003cth\u003e\u003cstrong\u003eSpecification\u003c\/strong\u003e\u003c\/th\u003e\n\u003c\/tr\u003e\n\u003c\/thead\u003e\n\u003ctbody\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eMinimum operating angle\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003e3°\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eEffective optical window diameter\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003eØ20 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eApplicable sample diameter\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003eØ20 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eOptical window material\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003eBeryllium (Be)\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eElectrode system\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003eThree-electroder\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eCell body material\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003eTi\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eInsulation material\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003ePEEK\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eCurrent collector tab\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003eGold-plated copper\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eReference electrode\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003eLithium wire\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cstrong\u003eCell body dimensions\u003c\/strong\u003e\u003c\/td\u003e\n\u003ctd\u003eØ49.5 mm × H23 mm\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp\u003e\u003cem\u003eNote: Solid beryllium is relatively stable and poses low skin-contact risk; avoid inhaling dust or aerosols and wash hands after handling.\u003cbr\u003e\u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0562\/5705\/2832\/files\/XRD-3E_dimensions_480x480.png?v=1787025287\" style=\"margin-bottom: 16px; float: none;\"\u003e\u003cbr\u003e\u003c\/em\u003e\u003c\/p\u003e\n\u003ch3\u003e\u003cspan\u003eInstrument Compatibility\u003c\/span\u003e\u003c\/h3\u003e\n\u003cp class=\"isSelectedEnd\"\u003e\u003cspan\u003e• \u003c\/span\u003e\u003cstrong\u003e\u003cspan\u003eXRD System Compatibility\u003c\/span\u003e\u003c\/strong\u003e\u003cbr\u003e\u003cspan\u003eCompatible with Bruker D8 systems and other X-ray diffractometers with suitable mounting and scan geometries. The sample holder, incident-angle range, beam path, and instrument clearance should be verified before testing\u003c\/span\u003e\u003c\/p\u003e\n\u003cp class=\"isSelectedEnd\"\u003e\u003cspan\u003e• \u003c\/span\u003e\u003cstrong\u003e\u003cspan\u003eElectrochemical Testing Compatibility\u003c\/span\u003e\u003c\/strong\u003e\u003cbr\u003e\u003cspan\u003eCompatible with commercial electrochemical workstations and battery testing systems that support three-electrode charge\/discharge testing\u003c\/span\u003e\u003c\/p\u003e\n\u003ch3\u003e\u003cspan\u003eOperando XRD Literature Example\u003c\/span\u003e\u003c\/h3\u003e\n\u003cp class=\"isSelectedEnd\"\u003e\u003cstrong\u003e\u003cspan\u003eOperando XRD Tracking of Graphite Lithiation\u003c\/span\u003e\u003c\/strong\u003e\u003c\/p\u003e\n\u003cp class=\"isSelectedEnd\"\u003e\u003cspan\u003eOlgo et al. studied a three-electrode graphite||NMC622 prismatic Li-ion cell using spatially resolved operando synchrotron XRD. The measurements tracked graphite staging transitions from graphite to LiC₁₂ and LiC₆. Compared with relatively uniform lithiation at C\/5, 2C charging caused delayed phase evolution and greater local heterogeneity. The stable LFP reference electrode enabled independent monitoring of graphite and NMC622 potentials while causing minimal disturbance to local lithiation behavior.\u003c\/span\u003e\u003c\/p\u003e\n\u003ch3\u003e\u003cspan\u003eDemonstrated Operando XRD Capabilities\u003c\/span\u003e\u003c\/h3\u003e\n\u003cul\u003e\n\u003cli\u003e\u003cspan\u003eIndependent monitoring of electrode potentials\u003c\/span\u003e\u003c\/li\u003e\n\u003cli\u003e\u003cspan\u003eOperando tracking of graphite → LiC₁₂ → LiC₆ transitions\u003c\/span\u003e\u003c\/li\u003e\n\u003cli\u003e\u003cspan\u003eDetection of rate-dependent lithiation heterogeneity\u003c\/span\u003e\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003cp class=\"isSelectedEnd\"\u003e\u003cem\u003e\u003cspan\u003e\u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0562\/5705\/2832\/files\/XRD-3E_e42375b0-a47f-46c6-baad-8a51901db187_480x480.png?v=1787025288\" style=\"margin-bottom: 16px; float: none;\"\u003e\u003c\/span\u003e\u003c\/em\u003e\u003c\/p\u003e\n\u003ch3\u003e\u003cspan\u003eApplication Studies\u003c\/span\u003e\u003c\/h3\u003e\n\u003cp\u003e\u003cspan\u003eApplication studies using this model are currently underway.\u003c\/span\u003e \u003c\/p\u003e\n\u003c\/div\u003e","brand":"Beyond Battery","offers":[{"title":"XRD-3E","offer_id":58301942988960,"sku":"CNB-12-XRD-3E","price":2203.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0562\/5705\/2832\/files\/XRD-3E_61088e48-67ec-450c-bbc8-8124247a105b.png?v=1787028631","url":"https:\/\/beyond-battery.com\/en-us\/products\/in-in-situ-xrd-battery-test-cell-model-xrd-3e","provider":"Beyond Battery","version":"1.0","type":"link"}